特集―分子性結晶のダイナミックス　新しい迅速Ｘ線回折装置による結晶構造解析の発展

• 植草 秀裕

  東京工業大学理学部化学科

書誌事項

タイトル別名

• Special Issue-Dynamics of Molecular Crystals. Recent Development of X-ray Crystal Structure Analysis by a New Diffractmeter for Rapid Data Collection.
• アタラシイ ジンソク Xセン カイセツ ソウチ ニ ヨル ケッショウ コウゾウ

抄録

Recently we designed and made a new no-screen Weissenberg camera type diffractometer for rapid data collection to determine the structures of reaction intermediates. The new features of the diffractometer are a κ-type goniometer, two imaging plates for recording and reading the intensity data, and spiral motion reading mechanism. The crystal mounted on a goniometer is aligned automatically and the three-dimensional intensity data were collected within two hours. Using this new diffractometer, we determined the structure of a syn-tricyclooctane derivative. The structure has not been analyzed with the four-circle diffratometer because the molecule easily reacts under X-ray irradiation .

収録刊行物

• 日本結晶学会誌

  日本結晶学会誌 37 (1), 42-47, 1995

  日本結晶学会

詳細情報

• CRID: 1390282679064419840
• NII論文ID: 10002023963
• NII書誌ID: AN00188364
• DOI: 10.5940/jcrsj.37.42
• ISSN: 18845576
• ISSN: 03694585
• NDL書誌ID: 3595186
• Web Site: https://ndlsearch.ndl.go.jp/books/R000000004-I3595186
• 本文言語コード: ja
• データソース種別:
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• 抄録ライセンスフラグ: 使用不可