Preparation of Acid Deficient Solutions of Uranyl Nitrate and Thorium Nitrate by Steam Denitration.
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- YAMAGISHI Shigeru
- Department of Chemistry and Fuel Research, Japan Atomic Energy Research Institute
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- TAKAHASHI Yoshihisa
- Department of Chemistry and Fuel Research, Japan Atomic Energy Research Institute
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Acid deficient heavy metal (HM) nitrate solutions are often required in the internal gelation processes for nuclear fuel fabrication. The stoichiometric HM-nitrate solutions are needed in a sol-gel process for fuel fabrication. A method for preparing such nitrate solutions with a controlled molar ratio of nitrate/metal by denitration of acid-excess nitrate solutions was developed. The denitration was conducted by bubbling a nitrate solution with a mixture of steam+Ar. It was found that steam was more effective for the denitration than Ar. The acid deficient uranyl nitrate solution with nitrate/U=1.55 was yielded by steam bubbling, while not by only Ar bubbling. As for thorium nitrate, acid deficient solutions of nitrate/Th ?? 3.1 were obtained by steam bubbling.
収録刊行物
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- Journal of Nuclear Science and Technology(日本原子力学会英文論文誌)
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Journal of Nuclear Science and Technology(日本原子力学会英文論文誌) 33 (2), 147-151, 1996
一般社団法人 日本原子力学会
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詳細情報 詳細情報について
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- CRID
- 1390001204095580288
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- NII論文ID
- 10002074221
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- NII書誌ID
- AA00703720
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- COI
- 1:CAS:528:DyaK28XhvVent70%3D
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- ISSN
- 18811248
- 00223131
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- 本文言語コード
- en
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- データソース種別
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- JaLC
- Crossref
- CiNii Articles
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- 抄録ライセンスフラグ
- 使用不可