機械的合金化したTi-hBN粉末中のBの状態分析 State Analysis of Boron in Mechanically Alloyed Ti-hBN Powder

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抄録

BK X-ray spectra from mechanically alloyed (MA) Ti-hBN powders were measured precisely using an electron probe microanalyzer (EPMA), in order to investigate the reaction progress of this system. Their spectra features were discussed in comparison with mechanically ground (MG) hBN oowders.<BR>At the early stage of MA, the main BK band at 6.9nm was almost unchanged, while 6.5nm satellite peak intensity was increased. From the result of milling of hBN alone, it was considered that hBN was changed into amorphous BN (aBN) in consequence of refinement, but B state of this aBN was still remained as same as that of hBN. BK spectra of 144ks MA powder was clearly different from that of TiB<SUB>2</SUB>, in spite of the observation of TiB<SUB>2</SUB> by X-ray diffraction measurement. This spectrum was in good agreement with the combined spectrum with aBN and TiB2 spectrum. In conclusion the excess of B was remained still as aBN after 144ks MA.

収録刊行物

  • 粉体および粉末冶金

    粉体および粉末冶金 43(11), 1300-1304, 1996-11-15

    Japan Society of Powder and Powder Metallurgy

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各種コード

  • NII論文ID(NAID)
    10002260952
  • NII書誌ID(NCID)
    AN00222724
  • 本文言語コード
    JPN
  • 資料種別
    ART
  • ISSN
    05328799
  • NDL 記事登録ID
    4077930
  • NDL 雑誌分類
    ZP41(科学技術--金属工学・鉱山工学)
  • NDL 請求記号
    Z17-274
  • データ提供元
    CJP書誌  NDL  J-STAGE 
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