Development of New In-House Grazing X-ray Reflection System for Analyzing Liquid Surface and Interface

  • Sato Shigeo
    Institute for Advanced Materials Processing, Tohoku University
  • Saito Masatoshi
    Institute for Advanced Materials Processing, Tohoku University
  • Matsubara Eiichiro
    Department of Materials Science and Engineering, Graduate School, Kyoto University
  • Waseda Yoshio
    Institute for Advanced Materials Processing, Tohoku University

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Abstract

An in-house grazing X-ray reflection (GXR) apparatus has been newly built for studying the liquid surface, and the liquid-solid and liquid-liquid interfaces. This apparatus consists of a high flux rotating anode X-ray generator, pairs of slits for incident and diffracted beams, a channel-cut Ge 440 crystal monochromator and a double-axis diffractometer. This system was tested by measuring X-ray reflectivity profiles from free surface of water or mercury, and the water-mercury interface.

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