Verification of Sandelin Phenomena in Mechanically Alloyed Fe-Zn and Fe-Zn-Si

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Mechanical alloying through the ball-milling of elemental powders to form the zinc-rich ζ binary Fe–Zn alloy, and the ternaries consisting of 0.12 mass%Si, 1.2 mass%Si, and 2.4 mass%Si, based on the same Fe/Zn ratio was performed. These materials have been designated as ζ, ζ+0.12 mass%Si, ζ+1.2 mass%Si, and ζ+2.4 mass%Si and mechanically alloyed to form their metastable states, η-Zn, FeSi and ζ phases. Differential scanning calorimetry (DSC) measurements of the materials show the presence of characteristic exothermic and endothermic reactions during their continuous transformation to stable equilibrium states. In the ζ+0.12 mass%Si material composition (i.e., Sandelin region), we observe an invariant reaction peak at around 422°C, corresponding to both the eutectic reaction in the Zn–Si and the melting of Zn in the Fe–Zn systems. The observation of the FeSi phase for all the compositions, while absent in coatings of Si bearing steels suggests a relationship between the Sandelin effect and its formation.

収録刊行物

  • Materials transactions, JIM

    Materials transactions, JIM 38(12), 1100-1105, 1997-12-01

    社団法人 日本金属学会

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各種コード

  • NII論文ID(NAID)
    10002454550
  • NII書誌ID(NCID)
    AA10699969
  • 本文言語コード
    ENG
  • 資料種別
    ART
  • ISSN
    09161821
  • NDL 記事登録ID
    4384541
  • NDL 雑誌分類
    ZP41(科学技術--金属工学・鉱山工学)
  • NDL 請求記号
    Z53-J286
  • データ提供元
    CJP書誌  NDL  J-STAGE 
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