Bulky Thiols and Their Coordination Compounds. An Improvement of the Removal Method of Tetrahydropyranyl Group from Thiols and Its Application for Ligand Syntheses

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  • Hideaki Watanabe
    Department of Chemistry, Faculty of Science, Science University of Tokyo
  • Seiji Ogo
    Department of Applied Molecular Science, Institute for Molecular Science
  • Takeshi Yamamura
    Department of Chemistry, Faculty of Science, Science University of Tokyo

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Abstract

<jats:title>Abstract</jats:title> <jats:p>The route for the syntheses of alkanthiols having bulky groups at the neighborhood of sulfur atoms was improved, and applied for the preparation of thiol ligands that mimic the cysteine containing metal binding sites in proteins. The new method developed the deprotection of tetrahydropyranyl group from α,α-diphenylalkyl 2-tetrahydropyranyl sulfides.</jats:p>

Journal

  • Chemistry Letters

    Chemistry Letters 25 (11), 999-1000, 1996-11-01

    Oxford University Press (OUP)

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