29Si and 1H NMR of Expandable Mica Ion-exchanged by NH4+

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<jats:title>Abstract</jats:title> <jats:p>The 29Si-NMR chemical shift of expandable mica ion-exchanged by NH4+ changes from −95 to −99.5 ppm after heat-treatment at 600 °C, which indicates a change from the mica to a talc structure. The 1H static NMR spectrum of protons remaining in the structure after heating showed a sharp signal with a full width at half maximum of 0.8 kHz at 1.0 ppm, which suggests a rapid proton motion in the structure.</jats:p>

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  • Chemistry Letters

    Chemistry Letters 26 (3), 199-200, 1997-03-01

    Oxford University Press (OUP)

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