Palladium-Catalyzed Coupling Polymerization of Bromophenylallenes and Sodium Malonates

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  • Nobuyuki Miyaki
    Research Laboratory of Resources Utilization, Tokyo Institute of TechnologyNagatuta-cho 4259, Midori-ku, Yokohama
  • Ikuyoshi Tomita
    Research Laboratory of Resources Utilization, Tokyo Institute of TechnologyNagatuta-cho 4259, Midori-ku, Yokohama
  • Takeshi Endo
    Research Laboratory of Resources Utilization, Tokyo Institute of TechnologyNagatuta-cho 4259, Midori-ku, Yokohama

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<jats:title>Abstract</jats:title> <jats:p>A trisubstituted poly(phenylene-vinylene) (Mn = 7700) was obtained in 67% yield by the coupling polymerization of p-bromophenylallene (1a) with sodium diethyl methylmalonate (2) at 80°C for 6h. Owing to the diethyl methylmalonate moieties in the side chain, the polymer is remarkably soluble in various organic solvents. From m-bromophenylallene (1b), a polymer was also obtained in high yield.</jats:p>

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  • Chemistry Letters

    Chemistry Letters 26 (8), 685-686, 1997-08-01

    Oxford University Press (OUP)

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