4,5-Diiodo-4′,5′-ethylenedioxytetrathiafulvalene and Its Metallic Radical Salts

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  • Yoshiyuki Kuwatani
    Department of Chemistry, Faculty of Science, Tokyo Metropolitan UniversityHachioji, Tokyo
  • Eiji Ogura
    Department of Chemistry, Faculty of Science, Tokyo Metropolitan UniversityHachioji, Tokyo
  • Hiroyuki Nishikawa
    Department of Chemistry, Faculty of Science, Tokyo Metropolitan UniversityHachioji, Tokyo
  • Isao Ikemoto
    Department of Chemistry, Faculty of Science, Tokyo Metropolitan UniversityHachioji, Tokyo
  • Masahiko Iyoda
    Department of Chemistry, Faculty of Science, Tokyo Metropolitan UniversityHachioji, Tokyo

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<jats:title>Abstract</jats:title> <jats:p>4,5-Diiodo-4′,5′-ethylenedioxy-TTF (EDO-TTFI2) was synthesized in moderate yield by the reaction of EDO-TTF with LDA, followed by quenching with CF3(CF2)5I. Although EDO-TTF contains electron-withdrawing iodine as the substituent, this compound has a similar donor ability to BEDT-TTF. The radical-cation salt (EDO-TTFI2)2·ClO4 shows a metallic conductivity down to 50 K, reflecting the strong I···O interaction.</jats:p>

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  • Chemistry Letters

    Chemistry Letters 26 (8), 817-818, 1997-08-01

    Oxford University Press (OUP)

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