The Formation of Monomethyl Carbonato-bridged Dinuclear Nickel(II)Complexes by an Efficient CO_2 Uptake in Methanol Containing Urea Derivatives

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Monomethyl carbonato-bridged dinuclear nickel(II) complexes [Ni<SUB>2</SUB>(L)(OOC-O-CH<SUB>3</SUB>)(CH<SUB>3</SUB>OH)<SUB>2</SUB>](ClO<SUB>4</SUB>)<SUB>2</SUB>·H<SUB>2</SUB>O·CH<SUB>3</SUB>OH, <B>1</B> and [Ni<SUB>2</SUB>(L)(OOC-O-CH<SUB>3</SUB>)(H<SUB>2</SUB>O)<SUB>2</SUB>](ClO<SUB>4</SUB>)<SUB>2</SUB>·H<SUB>2</SUB>O, <B>2</B> were obtained in the presence of [Ni<SUB>2</SUB>(L)(OH)(H<SUB>2</SUB>O)<SUB>2</SUB>](ClO<SUB>4</SUB>)<SUB>2</SUB> and <I>N</I>-methylurea at room temperature in air, where HL is <I>N</I>,<I>N</I>,<I>N′</I>,<I>N′</I>-tetrakis[(1-ethyl-2-benzimidazolyl)methyl]- 2-hydroxy-1,3-diaminopropane. The crystal structure of <B>1</B> was determined by X-ray crystallography and <B>2</B> was characterized by the magnetic susceptibility and visible absorption spectrum.

収録刊行物

  • Chemistry letters

    Chemistry letters 1997(9), 891-892, 1997-09

    The Chemical Society of Japan

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各種コード

  • NII論文ID(NAID)
    10002614780
  • NII書誌ID(NCID)
    AA00603318
  • 本文言語コード
    ENG
  • 資料種別
    ART
  • ISSN
    03667022
  • データ提供元
    CJP書誌  J-STAGE 
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