The Formation of Monomethyl Carbonato-bridged Dinuclear Nickel(II) Complexes by an Efficient CO2 Uptake in Methanol Containing Urea Derivatives

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  • Yoko Hosokawa
    Chemical Laboratory, Faculty of Education, Okayama UniversityTsushima-naka, Okayama
  • Heitaro Yamane
    Chemical Laboratory, Faculty of Education, Okayama UniversityTsushima-naka, Okayama
  • Yasuo Nakao
    Chemical Laboratory, Faculty of Education, Okayama UniversityTsushima-naka, Okayama
  • Keiji Matsumoto
    Department of Chemistry, Faculty of Science, Osaka City UniversitySumiyoshi-ku, Osaka
  • Satoshi Takamizawa
    Department of Chemistry, Graduate School of Science, Osaka UniversityMachikaneyama, Toyonaka, Osaka
  • Wasuke Mori
    Department of Chemistry, Faculty of Science, Kanagawa UniversityTsuchiya, Hiratsuka, Kanagawa
  • Shinnichiro Suzuki
    Department of Chemistry, Graduate School of Science, Osaka UniversityMachikaneyama, Toyonaka, Osaka

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<jats:title>Abstract</jats:title> <jats:p>Monomethyl carbonato-bridged dinuclear nickel(II) complexes [Ni2(L)(OOC-O-CH3)(CH3OH)2](ClO4)2·H2O·CH3OH, 1 and [Ni2(L)(OOC-O-CH3)(H2O)2](ClO4)2·H2O, 2 were obtained in the presence of [Ni2(L)(OH)(H2O)2](ClO4)2 and N-methylurea at room temperature in air, where HL is N,N,N′,N′-tetrakis[(1-ethyl-2-benzimidazolyl)methyl]- 2-hydroxy-1,3-diaminopropane. The crystal structure of 1 was determined by X-ray crystallography and 2 was characterized by the magnetic susceptibility and visible absorption spectrum.</jats:p>

収録刊行物

  • Chemistry Letters

    Chemistry Letters 26 (9), 891-892, 1997-09-01

    Oxford University Press (OUP)

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