New Pressure Domain in Single Crystal X-ray Diffraction Using a Sealed Source

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抄録

The pressure range of single crystal structure determination using a sealed source was extended to over 30 GPa with the improved techniques in this study. Rare gas solid helium was found to be the only pressure medium that can secure hydrostatic environment to very high pressure. The solid argon or neon induces significant divitoric stresses in crystals at relatively low pressure. The crystal volume was doubled at certain targeting pressure by using a new gasket material. The intrinsic background of a pressure cell was significantly reduced by a special collimator. These procedures improved the signal/noise ratio to 3 - 4 times. The quality of the structure refinement and the accuracy of atomic coordinates at 33 GPa are comparable with measurements at ambient conditions in a diamond cell.

収録刊行物

  • 高圧力の科学と技術 = The Review of high pressure science and technology

    高圧力の科学と技術 = The Review of high pressure science and technology 7, 145-147, 1998

    The Japan Society of High Pressure Science and Technology

参考文献:  7件中 1-7件 を表示

  • <no title>

    FUJISHIRO I.

    Proc. of the 8th AIRAPT Conf. 608, 1981

    被引用文献1件

  • <no title>

    BELL P. M.

    Annual report of Geophysical Laboratory, Carnegie institution of Washington, 404-406, 1980

    被引用文献1件

  • <no title>

    HAZEN R.

    Am. Mineral. 74, 352-359, 1989

    被引用文献1件

  • <no title>

    DOWNS R. T.

    Am. Mineral. 81, 51-55, 1996

    被引用文献1件

  • X-ray Diffraction on Single Crystals at High pressure

    AHSBAHS H.

    Prog. Cryst. Growth and Charact. 14, 263-302, 1987

    被引用文献2件

  • <no title>

    DOWNS R. T.

    Am. Mineral. 79, 1042-1052, 1994

    被引用文献1件

  • <no title>

    ROSS N. L.

    Am. Miner. 75, 739-747, 1990

    被引用文献6件

各種コード

  • NII論文ID(NAID)
    10002689121
  • NII書誌ID(NCID)
    AN10452913
  • 本文言語コード
    ENG
  • 資料種別
    ART
  • ISSN
    0917639X
  • NDL 記事登録ID
    4493862
  • NDL 雑誌分類
    ZP1(科学技術--化学・化学工業)
  • NDL 請求記号
    Z17-1589
  • データ提供元
    CJP書誌  NDL  J-STAGE 
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