New Synthesis Technique for Making Hydroxyapatite Ceramics Using Hydrothermal Hot-Pressing.

  • Hosoi K.
    Shiraishi Central Laboratories Co. Ltd.
  • Korenaga T.
    Shiraishi Central Laboratories Co. Ltd.
  • Hashida T.
    Research Institute for Fracture Technology, Tohoku University
  • Takahashi H.
    Research Institute for Fracture Technology, Tohoku University
  • Yamasaki N.
    Research Laboratory of Hydrothermal Chemistry, Kochi University

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  • New Synthesis Technique for Making Hydr

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Abstract

A new synthesis technique for making hydroxyapatite (HAp) ceramics has been developed using hydrothermal hotpressing (HHP) method at relatively low temperature below 150°C. Powder mixture of dibasic calcium phosphate dihydrate and calcium hydroxide with the Ca/P ratio of 1. 67 was treated at 150°C and 40MPa. The resulted solidified body could be identified as HAp by X-ray diffraction (XRD) analysis. Moreover we tried to prepare Chitosan-HAp composite for practical utilization of low-temperature-process. Chitosan-HAp composite was improved the tensile strength twice times and over up as compared with plain HAp ceramics.

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