Synthesis of (−)-Gleenol via C-H Insertion Reaction of Alkylidenecarbene

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  • Susumu Ohira
    Department of Biological Chemistry, Faculty of Science, Okayama University of Science
  • Naoya Yoshihara
    Department of Biological Chemistry, Faculty of Science, Okayama University of Science
  • Taisuke Hasegawa
    Department of Biological Chemistry, Faculty of Science, Okayama University of Science

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<jats:title>Abstract</jats:title> <jats:p>A spiro sesquiterpene alcohol, (−)-gleenol (1) was synthesized from (−)-l-menthol in 16 steps, using the C-H insertion reaction of the alkylidenecarbene as the key step. The absolute configuration of (−)-1 was determined to be 1S, 6R, 7S, 10R.</jats:p>

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  • Chemistry Letters

    Chemistry Letters 27 (8), 739-740, 1998-08-01

    Oxford University Press (OUP)

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