Highly Diastereoselective Aldol Synthesis from <i>α</i>-Iodo Ketones in Aqueous Media

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  • Ikuya Shibata
    Department of Applied Chemistry, Fuculty of Engineering, Osaka University2-1 Yamadaoka, Suita, Osaka
  • Masatsugu Kawasaki
    Department of Applied Chemistry, Fuculty of Engineering, Osaka University2-1 Yamadaoka, Suita, Osaka
  • Makoto Yasuda
    Department of Applied Chemistry, Fuculty of Engineering, Osaka University2-1 Yamadaoka, Suita, Osaka
  • Akio Baba
    Department of Applied Chemistry, Fuculty of Engineering, Osaka University2-1 Yamadaoka, Suita, Osaka

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<jats:title>Abstract</jats:title> <jats:p>Highly diastereoselective aldol synthesis from α-iodo ketones was promoted under aqueous conditions by a distannane system, (n-Bu3Sn)2, n-Bu2SnF2 and HMPA. Aqueous solutions of acetaldehyde, formaldehyde and pivaraldehyde were applicable to give β-hydroxy ketones effectively.</jats:p>

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  • Chemistry Letters

    Chemistry Letters 28 (7), 689-690, 1999-07-01

    Oxford University Press (OUP)

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