Analysis of Pressure Sensitive Adhesives by GC/MS and GC/AED with Temperature Programmable Pyrolyzer

この論文にアクセスする

この論文をさがす

著者

抄録

Gas chromatograph/mass spectrometer (GC/MS) and gas chromatograph/atomic emission detector (GC/AED) with temperature programmable pyrolyzer were used for analysis of pressure sensitive adhesives in adhesive tapes. Evolved gas analysis (EGA) profile of the adhesives was obtained by this temperature-programmed pyrolyzer directly coupled with MS via a deactivated metal capillary tube. The EGA profile suggested the optimal thermal desorption condition for additives and the subsequent optimal pyrolysis temperature for the remaining polymeric material. Rubbers were identified from pyrograms with the assistance of a new polymer library. The additives were selectively detected by monitoring hetero elements and these screening results of GC/AED enabled one to easily find additive peaks in complex chromatograms of GC/MS with interference of tackifier. The additives were able to be identified by the corresponding GC/MS data. Furthermore, the EGA profile gave significant data for crosslinking agents by using specific ion monitoring.

収録刊行物

  • Analytical sciences : the international journal of the Japan Society for Analytical Chemistry

    Analytical sciences : the international journal of the Japan Society for Analytical Chemistry 16(6), 627-631, 2000-06-10

    社団法人 日本分析化学会

参考文献:  9件中 1-9件 を表示

  • <no title>

    WATANABE C.

    High Polymers Jpn. 43, 110, 1994

    被引用文献1件

  • <no title>

    SATO H.

    Macromolecules 30, 4030, 1997

    被引用文献3件

  • <no title>

    WATANABE C.

    J. High Resolut. Chromatogr. 14, 269, 1991

    被引用文献3件

  • <no title>

    OHTANI H.

    J. Anal. Appl. Pyrolysis 25, 1, 1993

    被引用文献6件

  • <no title>

    WYLIE P. L.

    J.High Resolut.Chromatogr. 12, 813, 1989

    被引用文献2件

  • <no title>

    SULLIVAN J. J.

    Anal.Chem. 62, 1035, 1990

    被引用文献1件

  • <no title>

    WYLIE P. L.

    J.High Resolut.Chromatogr. 13, 499, 1990

    被引用文献2件

  • <no title>

    ITO S.

    J.Mass Spectrom.Soc.Jpn. 46, 336, 1998

    被引用文献1件

  • <no title>

    SATO H.

    J.Anal.Appl.Pyrolysis 37, 173, 1996

    DOI 被引用文献3件

各種コード

  • NII論文ID(NAID)
    10004955194
  • NII書誌ID(NCID)
    AA10500785
  • 本文言語コード
    ENG
  • 資料種別
    ART
  • ISSN
    09106340
  • NDL 記事登録ID
    5380278
  • NDL 雑誌分類
    ZP4(科学技術--化学・化学工業--分析化学)
  • NDL 請求記号
    Z54-F482
  • データ提供元
    CJP書誌  NDL  J-STAGE 
ページトップへ