書誌事項
- タイトル別名
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- Relationship between Crystallographic Structure of Electrodeposited Ni-P AlloyFilm and Its Thermal Equilibrium Diagram
- デンセキNi P ゴウキンメッキ マク ノ ビサイ コウゾウ ト ネツ ヘイコウ ジョウタイズ ト ノ カンケイ
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The electrodeposited Ni-P alloy films were obtained from Watts baths containing H3PO3. The crystallographic structure and morphology of electrodeposited Ni-P films were studied by using XRD, HRTEM, SEM and heat-treatment technique. The crystallographic structures of electrodeposited Ni-P alloy films was also compared with the Ni-P thermal equilibrium diagram. <BR>The X-ray diffraction patterns of Ni-P electrodeposited films with various P contents gradually changed from sharp peaks to broad peaks with increasing P contents in electrodeposited films. HRTEM observation revealed that the crystallographic structure of electrodeposited Ni-P film with 18.5 at%P content was crystalline and its crystal size was about 10 nm. Moreover, the crystalline structure was observed and the crystal size was about 3 nm in the electrodeposited Ni-P alloy film with 21.5 at%P content. However, when the film with 21.5 at%P content was heat treated, the crystalline phase did not grow and Ni3P existed alone under 300°C heat-treatment. From this result, it was clear that the crystallographic structure of Ni-P film with 21.5 at%P content was amorphous. <BR>Therefore, it can be concluded that the microcrystalline phase existed up to 19 at%P in electrodeposited Ni-P alloy film and the amorphous phase existed from 19 at% to 32 at%P.
収録刊行物
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- 日本金属学会誌
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日本金属学会誌 65 (6), 495-501, 2001
公益社団法人 日本金属学会
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詳細情報 詳細情報について
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- CRID
- 1390001206491334656
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- NII論文ID
- 130007341882
- 10006543916
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- NII書誌ID
- AN00187860
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- ISSN
- 18806880
- 24337501
- 00214876
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- NDL書誌ID
- 5823988
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- データソース種別
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- JaLC
- NDL
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