The Rhodium(II) Acetate- Catalyzed Reaction of Alkenyl and Alkynyl α-Diazoacetates with Thioketene

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The reaction of allyl <i>α</i>-diazoacetates with di-<i>t</i>-butylthioketene catalyzed by Rh<sub>2</sub>(OAc)<sub>4</sub> gave 4-allyl-2-methylene-1,3-oxathiolan-5-ones through the 1,5-cyclization of a thiocarbonyl ylide intermediate followed by Claisen rearrangement with allene episulfide through the 1,3-cyclization of the intermediate. Other alkenyl and alkynyl diazoacetates also gave similar products through the thiocarbonyl ylide without affording its intramolecular 1,3-dipolar cycloadduct.

収録刊行物

  • Bulletin of the Chemical Society of Japan

    Bulletin of the Chemical Society of Japan 68(5), 1393-1400, 1995-05-15

    The Chemical Society of Japan

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各種コード

  • NII論文ID(NAID)
    10008889723
  • NII書誌ID(NCID)
    AA00580132
  • 本文言語コード
    ENG
  • 資料種別
    ART
  • ISSN
    00092673
  • データ提供元
    CJP書誌  J-STAGE 
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