Ruthenium Complex-catalyzed Oxidative Cyclization of 4-Penten-1-ols

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著者

    • KONDO Teruyuki
    • Department of Energy and Hydrocarbon Chemistry, Graduate School of Engineering, Kyoto University
    • TSUNAWAKI Fumiaki
    • Department of Energy and Hydrocarbon Chemistry, Graduate School of Engineering, Kyoto University
    • SATO Ryosuke
    • Department of Energy and Hydrocarbon Chemistry, Graduate School of Engineering, Kyoto University
    • URA Yasuyuki
    • Department of Energy and Hydrocarbon Chemistry, Graduate School of Engineering, Kyoto University
    • WADA Kenji
    • Department of Energy and Hydrocarbon Chemistry, Graduate School of Engineering, Kyoto University
    • MITSUDO Take-aki
    • Department of Energy and Hydrocarbon Chemistry, Graduate School of Engineering, Kyoto University

抄録

Treatment of 2-phenyl-5-hexen-2-ol (<B>1a</B>) with Ru<SUB>3</SUB>(CO)<SUB>12</SUB> catalyst and PPh<SUB>3</SUB> ligand in the presence of allyl acetate and K<SUB>2</SUB>CO<SUB>3</SUB> in toluene at 160 °C for 20 h under 5 atm of carbon monoxide gave the corresponding oxidative cyclization product, 2,5-dimethyl-2-phenyl-2,3-dihydrofuran (<B>2a</B>), in quantitative yield (>99%).

収録刊行物

  • Chemistry letters

    Chemistry letters 32(1), 24-25, 2003-01-05

    The Chemical Society of Japan

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各種コード

  • NII論文ID(NAID)
    10012812910
  • NII書誌ID(NCID)
    AA00603318
  • 本文言語コード
    ENG
  • 資料種別
    SHO
  • ISSN
    03667022
  • データ提供元
    CJP書誌  J-STAGE 
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