η^3-Coordination of Hexadentate N, N, N', N'-Tetrakis(2-pyridylmethyl)ethylenediamine (tpen) to a Mononuclear fac-Re ^<VII>O_3 Center. The Isolation of a New Class of Metal-containing Ligands

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著者

    • MITANI Ayako
    • Division of Chemistry, Graduate School of Science, Hokkaido University
    • ABE Masaaki
    • Division of Chemistry, Graduate School of Science, Hokkaido University
    • TSUGE Kiyoshi
    • Division of Chemistry, Graduate School of Science, Hokkaido University
    • SASAKI Yoichi
    • Division of Chemistry, Graduate School of Science, Hokkaido University

抄録

Reaction of Re<SUP>V</SUP>OCl<SUB>3</SUB>(PPh<SUB>3</SUB>)<SUB>2</SUB> with an equimolar amount of tpen affords <I>fac</I>-[Re<SUP>VII</SUP>O<SUB>3</SUB>(η<SUP>3</SUP>-tpenH)](ClO<SUB>4</SUB>)<SUB>2</SUB> (<B>1</B>), in which the tpen ligand coordinates to the <I>fac</I>-Re<SUP>VII</SUP>O<SUB>3</SUB> center in a η<SUP>3</SUP>-mode, and the dangling bis(2-pyridylmethyl)amine arm in <B>1</B> is subsequently used to produce a heterobimetallic complex <I>fac</I>-, <I>fac</I>-[Re<SUP>VII</SUP>O<SUB>3</SUB>(μ-η<SUP>3</SUP>:η<SUP>3</SUP>-tpen)Re<SUP>I</SUP>(CO)<SUB>3</SUB>](ClO<SUB>4</SUB>)<SUB>2</SUB>.

収録刊行物

  • Chemistry letters

    Chemistry letters 32(6), 502-503, 2003-06-05

    The Chemical Society of Japan

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各種コード

  • NII論文ID(NAID)
    10012816701
  • NII書誌ID(NCID)
    AA00603318
  • 本文言語コード
    ENG
  • 資料種別
    SHO
  • ISSN
    03667022
  • データ提供元
    CJP書誌  J-STAGE 
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