Synthesis of Stannole Anion by Alkylation of Stannole Dianion

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  • Masaichi Saito
    Department of Chemistry, Faculty of Science, Saitama UniversityShimo-okubo, Sakura-ku, Saitama
  • Ryuta Haga
    Department of Chemistry, Faculty of Science, Saitama UniversityShimo-okubo, Sakura-ku, Saitama
  • Michikazu Yoshioka
    Department of Chemistry, Faculty of Science, Saitama UniversityShimo-okubo, Sakura-ku, Saitama

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Abstract

<jats:title>Abstract</jats:title> <jats:p>Reaction of tert-butylchloride with the stannole dianion first and simply prepared by the reduction of 1,1,2,3,4,5-hexaphenylstannole with lithium in ether gave 1-tert-butylstannole anion which was characterized by 1H, 13C, 119Sn, and 7Li NMR spectra and whose reactivities were investigated.</jats:p>

Journal

  • Chemistry Letters

    Chemistry Letters 32 (10), 912-913, 2003-09-08

    Oxford University Press (OUP)

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