Analytical Method for Determining Iminoctadine Triacetate by LC/ESI/MS Using Hydrophilic Interaction Chromatography

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著者

    • YANO Miho
    • Hyogo Prefectural Institute of Public Health and Environmental Sciences
    • MAKIHATA Nobuko
    • Hyogo Prefectural Institute of Public Health and Environmental Sciences

抄録

A target value for iminoctadine triacetate residues in tap water was set at 6 µg/l in Japan. We have developed a highly selective and sensitive analytical method for iminoctadine triacetate by solid phase extraction LC/ESI/MS using hydrophilic interaction chromatography. The recovery rates at concentration of 0.06, 0.6, and 6 µg/l in distilled water, tap water, and raw water were 77.1 - 96.7%, and CV were 3.7 - 13.2%. The quantitation limit of the present method was 0.04 µg/l, and it was able to measure even one-hundredth of the target value of iminoctadine triacetate quantitatively.

収録刊行物

  • Analytical sciences : the international journal of the Japan Society for Analytical Chemistry  

    Analytical sciences : the international journal of the Japan Society for Analytical Chemistry 22(4), 489-490, 2006-04-10 

    The Japan Society for Analytical Chemistry

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被引用文献:  3件

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各種コード

  • NII論文ID(NAID)
    10018123364
  • NII書誌ID(NCID)
    AA10500785
  • 本文言語コード
    ENG
  • 資料種別
    SHO
  • ISSN
    09106340
  • データ提供元
    CJP書誌  CJP引用  J-STAGE 
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