Analytical Method for Determining Iminoctadine Triacetate by LC/ESI/MS Using Hydrophilic Interaction Chromatography
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- KAWAMOTO Tatsuhiko
- Hyogo Prefectural Institute of Public Health and Environmental Sciences
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- YANO Miho
- Hyogo Prefectural Institute of Public Health and Environmental Sciences
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- MAKIHATA Nobuko
- Hyogo Prefectural Institute of Public Health and Environmental Sciences
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抄録
A target value for iminoctadine triacetate residues in tap water was set at 6 µg/l in Japan. We have developed a highly selective and sensitive analytical method for iminoctadine triacetate by solid phase extraction LC/ESI/MS using hydrophilic interaction chromatography. The recovery rates at concentration of 0.06, 0.6, and 6 µg/l in distilled water, tap water, and raw water were 77.1 - 96.7%, and CV were 3.7 - 13.2%. The quantitation limit of the present method was 0.04 µg/l, and it was able to measure even one-hundredth of the target value of iminoctadine triacetate quantitatively.
収録刊行物
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- Analytical Sciences
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Analytical Sciences 22 (4), 489-490, 2006
社団法人 日本分析化学会
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詳細情報
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- CRID
- 1390001204255807104
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- NII論文ID
- 10018123364
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- NII書誌ID
- AA10500785
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- ISSN
- 13482246
- 09106340
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- 本文言語コード
- en
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- データソース種別
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- JaLC
- Crossref
- CiNii Articles
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- 抄録ライセンスフラグ
- 使用不可