無電解ニッケルめっきを用いた微小ディスク電極プローブの作製 Fabrication of Micro-disk Electrode Probe by Electroless Nickel Plating

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Fabrication of the micro-disk electrode probe, which is convenient for micro-electrochemistry of localized surfaces or in small amounts of solution, has required special equipment or technical skills. In order to fabricate a micro-disk electrode probe simply, nickel electroless plating in a glass pipette was applied. After activation of the inside of a glass pipette heated and pulled off, nickel electroless-plating solution was successively introduced to deposit nickel in the pipette. Polishing the tip of the pipette and/or electroplating Ni, Cu or Pt obtained a disk surface with a diameter less than a few tens of micrometers. Cyclic voltammetry of the disk electrode showed a sigmoid curve and gave a limiting current which was identical with the theoretical value as a micro-disk electrode, indicating that this method was promising for fabrication of micro-disk electrodes. The electroless-plating micro-disk electrode was employed as a probe for scanning electrochemical microscopy to demonstrate its performance.<br>

収録刊行物

  • 表面技術 = The Journal of the Surface Finishing Society of Japan

    表面技術 = The Journal of the Surface Finishing Society of Japan 57(8), 592-596, 2006-08-01

    The Surface Finishing Society of Japan

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各種コード

  • NII論文ID(NAID)
    10018208744
  • NII書誌ID(NCID)
    AN1005202X
  • 本文言語コード
    JPN
  • 資料種別
    ART
  • ISSN
    09151869
  • NDL 記事登録ID
    8066465
  • NDL 雑誌分類
    ZP41(科学技術--金属工学・鉱山工学)
  • NDL 請求記号
    Z17-291
  • データ提供元
    CJP書誌  NDL  J-STAGE 
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