Crystallization of Ergosterol from Hexane Solution by a Continuous Column Crystallizer Equipped with a Water Feeding System
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- Kawachi Hideo
- Department of Applied and Bioapplied Chemistry, Graduate School of Engineering, Osaka City University
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- Ooshima Hiroshi
- Department of Applied and Bioapplied Chemistry, Graduate School of Engineering, Osaka City University
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Ergosterol was crystallized from hexane solution by using a novel continuous column crystallizer equipped with a water feeding system. The water feeding system was used to control the water concentration of the crystallization solution at a ppm-level. Precipitates recovered from the bottom of the crystallizer were agglomerates that were a mixture of amorphous solid and monohydrate micro crystals. The water concentration of the crystallization solution played an important role for the size and the crystallinity of the precipitates. Large precipitates having a good filtration property were recovered when the water concentration of the solution was 162 ppm, namely when the mole ratio of water to ergosterol was 0.89.
収録刊行物
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- JOURNAL OF CHEMICAL ENGINEERING OF JAPAN
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JOURNAL OF CHEMICAL ENGINEERING OF JAPAN 39 (11), 1200-1205, 2006
公益社団法人 化学工学会
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詳細情報 詳細情報について
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- CRID
- 1390001204567368576
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- NII論文ID
- 10018401733
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- NII書誌ID
- AA00709658
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- ISSN
- 18811299
- 00219592
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- NDL書誌ID
- 8553618
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- 本文言語コード
- en
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- データソース種別
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- JaLC
- NDL
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- 使用不可