Iron-catalyzed Direct-type Hydroxymethylation of 1,3-Dicarbonyl Compounds in Water
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Direct-type hydroxymethylation of 1,3-dicarbonyl compounds with aqueous formaldehyde proceeded smoothly in water in the presence of Fe(NO<SUB>3</SUB>)<SUB>3</SUB>·9H<SUB>2</SUB>O and sodium dodecylbenzenesulfate (SDBS), to afford the corresponding products in good to high yields.
- Chemistry Letters
Chemistry Letters 36(1), 56-57, 2007-01-05
The Chemical Society of Japan