Control of β-Tricalcium Phosphate Formation in Macroporous Phosphate Glass-Ceramic Composites
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- Obata Akiko
- Department of Materials Science and Engineering, Graduate School of Engineering, Nagoya Institute of Technology
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- Sasaki Megumi
- Department of Materials Science and Engineering, Graduate School of Engineering, Nagoya Institute of Technology
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- Kasuga Toshihiro
- Department of Materials Science and Engineering, Graduate School of Engineering, Nagoya Institute of Technology
書誌事項
- タイトル別名
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- Control of β-Tricalcium Phosphate Formation in Macroporous Phosphate Glass-Ceramic Composites
- Control of ベータ Tricalcium Phosphate Formation in Macroporous Phosphate Glass Ceramic Composites
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A macroporous phosphate invert glass-ceramic (PIGC) was derived from the mother glass with a composition of 60CaO-30P2O5-3TiO2-7Na2O in mol%. The mother glass powders were coated on a polymer sponge skeleton and subsequently sintered at 850°C for 1 h through burning off the sponge, resulting in the preparation of macroporous PIGC. The resulting macroporous PIGC consists predominantly of β-tricalcium phosphate (β-TCP) and β-calcium pyrophosphate and has large-sized pores of 300–1000 μm in diameter and small-sized pores of several tens micrometer in diameter. A new type of composite containing a large amount of β-TCP was also prepared by heating the mixture of the mother glass powders with Ca(OH)2 at 800°C for 1 h. The amount of β-TCP in the crystalline phase of the composites increased with increasing the Ca(OH)2 amount. The β-TCP-containing glass-ceramic composites can be prepared by firing at a considerably lower temperature than a conventional β-TCP ceramics. The amount of β-TCP in the composites is controllable by variation of the Ca(OH)2 amount. The composites showed higher solubility in an acetic acid solution at 37°C with an initial pH value of 5.0 in comparison with PIGC. The solubility of one of the composites was comparable with that of pure β-TCP. The composites are expected to be applicable for biodegradable scaffold for bone tissue engineering.
収録刊行物
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- MATERIALS TRANSACTIONS
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MATERIALS TRANSACTIONS 48 (3), 313-316, 2007
公益社団法人 日本金属学会
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詳細情報 詳細情報について
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- CRID
- 1390001204251936256
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- NII論文ID
- 130004453462
- 10018734219
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- NII書誌ID
- AA1151294X
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- ISSN
- 13475320
- 13459678
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- NDL書誌ID
- 8670383
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- 本文言語コード
- en
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- データソース種別
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- JaLC
- NDL
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