Growth of β-Perylene Crystal

  • Tomoaki Yago
    National Institute of Advanced Industrial Science and Technology (AIST)
  • Yoshiaki Tamaki
    National Institute of Advanced Industrial Science and Technology (AIST)
  • Akihiro Furube
    National Institute of Advanced Industrial Science and Technology (AIST)
  • Ryuzi Katoh
    National Institute of Advanced Industrial Science and Technology (AIST)

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<jats:title>Abstract</jats:title> <jats:p>Although perylene crystals have been known to show both dimeric (α) and monomeric (β) phases, to date only the stable α-crystals have been obtained under conventional conditions. Here, we propose a procedure for the selective growth of β-phase perylene crystals, in which a saturated toluene solution at 350 K was cooled to 298 K with a high cooling rate (−30 K/min). The sizes of β-phase crystals obtained were in the order of 100 μm.</jats:p>

収録刊行物

  • Chemistry Letters

    Chemistry Letters 36 (3), 370-371, 2007-02-03

    Oxford University Press (OUP)

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