A Novel S-bridged Pd^<II>_2Hg^<II> Metallacycle of D-Penicillaminate that Forms a Unique Supramolecular Structure Combined with Tetraamminepalladium(II)

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The newly prepared [Hg(<FONT SIZE="-2">D</FONT>-Hpen-<I>S</I>)(<FONT SIZE="-2">D</FONT>-H<SUB>2</SUB>pen-<I>S</I>)]<SUP>+</SUP> (<FONT SIZE="-2">D</FONT>-H<SUB>2</SUB>pen = <FONT SIZE="-2">D</FONT>-penicillamine) reacted with [PdBr<SUB>4</SUB>]<SUP>2−</SUP> in aqueous ammonia to give a Pd<SUP>II</SUP><SUB>2</SUB>Hg<SUP>II</SUP> cyclic complex, [Pd<SUB>2</SUB>HgBr<SUB>2</SUB>(<FONT SIZE="-2">D</FONT>-pen-<I>N</I>,<I>S</I>)<SUB>3</SUB>(NH<SUB>3</SUB>)]<SUP>2−</SUP>, by way of a Pd<SUP>II</SUP><SUB>3</SUB> cyclic complex, [Pd<SUB>3</SUB>(<FONT SIZE="-2">D</FONT>-pen-<I>N</I>,<I>O</I>,<I>S</I>)<SUB>3</SUB>]. The Pd<SUP>II</SUP><SUB>2</SUB>Hg<SUP>II</SUP> complex was found to aggregate into a cylindrical supramolecular structure in combination with [Pd(NH<SUB>3</SUB>)<SUB>4</SUB>]<SUP>2+</SUP>, accommodating [HgBr<SUB>3</SUB>(NH<SUB>3</SUB>)]<SUP>−</SUP> in its cavity.

収録刊行物

  • Chemistry letters

    Chemistry letters 36(3), 434-435, 2007-03-05

    The Chemical Society of Japan

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各種コード

  • NII論文ID(NAID)
    10018829905
  • NII書誌ID(NCID)
    AA00603318
  • 本文言語コード
    ENG
  • 資料種別
    SHO
  • ISSN
    03667022
  • データ提供元
    CJP書誌  J-STAGE 
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