Acetyl Chloride-Mediated Synthesis of trans-2-[(Diethoxyphosphorylamino)alkyl]-4-aryl-5,5-dimethyl-1,3,2λ^5-dioxaphosphorinane-2-oxide

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著者

    • Miao Zhiwei MIAO Zhiwei
    • State Key Laboratory of Elemento-Organic Chemistry, Research Institute of Elemento-Organic Chemistry, Nankai University
    • CHEN Ruyu
    • State Key Laboratory of Elemento-Organic Chemistry, Research Institute of Elemento-Organic Chemistry, Nankai University

抄録

<I>N</I>-Phosphoramino-protected six-membered cyclic α-aminophosphonates <I>trans</I>-2-[(diethoxyphosphorylamino)alkyl]-4-aryl-5,5-dimethyl-1,3,2λ<SUP>5</SUP>-dioxaphosphorinane-2-oxide <B>4a</B>–<B>4l</B> were synthesized with the help of acetyl chloride. <SUP>31</SUP>P NMR was used to trace the reaction process. A possible reaction mechanism was proposed and the stereochemistry of the title compounds was studied. In order to confirm the structure of <B>4</B>, products <B>4f</B> and <B>4k</B> were recrystallized and determined by X-ray diffraction analysis.

収録刊行物

  • Bulletin of the Chemical Society of Japan

    Bulletin of the Chemical Society of Japan 81(5), 630-635, 2008-05-15

    The Chemical Society of Japan

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各種コード

  • NII論文ID(NAID)
    10021075624
  • NII書誌ID(NCID)
    AA00580132
  • 本文言語コード
    ENG
  • 資料種別
    ART
  • ISSN
    00092673
  • NDL 記事登録ID
    9489837
  • NDL 雑誌分類
    ZP1(科学技術--化学・化学工業)
  • NDL 請求記号
    Z53-B35
  • データ提供元
    CJP書誌  NDL  J-STAGE 
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