Sulfur-assisted Fabrication of Silicon Nitride Nanorods in Autoclaves at 250℃

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著者

    • YANG Lishan
    • Key Laboratory of Colloid and Interface Chemistry, Shandong University, Ministry of Education
    • GUO Chunli
    • Key Laboratory of Colloid and Interface Chemistry, Shandong University, Ministry of Education
    • WANG Liancheng
    • Key Laboratory of Colloid and Interface Chemistry, Shandong University, Ministry of Education
    • BAI Zhongchao
    • Key Laboratory of Colloid and Interface Chemistry, Shandong University, Ministry of Education
    • FU Li
    • Key Laboratory of Colloid and Interface Chemistry, Shandong University, Ministry of Education
    • MA Xiaojian
    • Key Laboratory of Colloid and Interface Chemistry, Shandong University, Ministry of Education
    • XU Liqiang
    • Key Laboratory of Colloid and Interface Chemistry, Shandong University, Ministry of Education
    • QIAN Yitai
    • Key Laboratory of Colloid and Interface Chemistry, Shandong University, Ministry of Education

抄録

Silicon nitride nanorods were fabricated from Si, NaN<SUB>3</SUB>, and sulfur powder at 250 °C. XRD patterns show that the final product is mixed α- and β-Si<SUB>3</SUB>N<SUB>4</SUB>. SEM, TEM, and HRTEM images reveal that the product was composed of crystalline Si<SUB>3</SUB>N<SUB>4</SUB> nanorods with diameters in the range of 70–400 nm and lengths up to 3 μm. It is found that sulfur plays a crucial role in the low-temperature formation of Si<SUB>3</SUB>N<SUB>4</SUB> powders. Low reaction temperature and cheap raw materials make it possible for large scale synthesis of Si<SUB>3</SUB>N<SUB>4</SUB> nanomaterials.

収録刊行物

  • Chemistry letters

    Chemistry letters 37(3), 302-303, 2008-03-05

    公益社団法人 日本化学会

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各種コード

  • NII論文ID(NAID)
    10021078492
  • NII書誌ID(NCID)
    AA00603318
  • 本文言語コード
    ENG
  • 資料種別
    SHO
  • ISSN
    03667022
  • データ提供元
    CJP書誌  J-STAGE 
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