GC/MSによる魚介類中の農薬一斉分析法の検討 Investigation on Comprehensive Analysis of Pesticides in Fish and Shellfish by GC/MS

この論文にアクセスする

この論文をさがす

著者

抄録

A simple pretreatment of sample and comprehensive analysis method has been developed for the GC/MS determination of 29 pesticides in fish and shellfish. For the pretreatment, the pesticides in the sample were extracted with acetonitrile and the lipid in the sample extract was eliminated by partitioning between hexane and acetonitrile. After Sep-Pak Plus Florisil or Florisil PR column clean-up, the sample extract was analyzed by GC/MS (SIM). Recovery tests were performed by use of Sep-Pak Plus Florisil and Florisil PR for fish and shellfish. On the whole, recoveries (%) and CV (%) by Florisil PR were better than those by Sep-pak Plus Florisil in both of Japanese smelt (fish) and corbicula (shellfish). However, Sep-Pak Plus Florisil had better results in pyrokiron, fenthion, etc., so selection of clean-up procedure in agreement with the purpose was recommended. The quantification limits were 0.002∼0.005μg/g for most of the 29 pesticides.

収録刊行物

  • 環境化学 : journal of environmental chemistry

    環境化学 : journal of environmental chemistry 18(2), 227-235, 2008-06-24

    Japan Society for Environmental Chemistry

参考文献:  4件中 1-4件 を表示

キーワード

各種コード

  • NII論文ID(NAID)
    10021084992
  • NII書誌ID(NCID)
    AN10547099
  • 本文言語コード
    JPN
  • 資料種別
    NOT
  • ISSN
    09172408
  • NDL 記事登録ID
    9554614
  • NDL 雑誌分類
    ZN5(科学技術--建設工学・建設業--都市工学・衛生工学) // ZP1(科学技術--化学・化学工業)
  • NDL 請求記号
    Z16-2322
  • データ提供元
    CJP書誌  NDL  J-STAGE 
ページトップへ