An Accurate Quantitative Analysis of Polymorphic Content by Chemometric X-ray Powder Diffraction

この論文にアクセスする

この論文をさがす

著者

抄録

Data from X-ray powder diffraction (XRD) were subjected to a partial least-squares regression analysis (PLS) to build a calibration model for predicting the polymorphic content of carbamazepine (CBZ). The effectiveness of the PLS method in the construction of calibration models was analyzed by a scientific approach based on a regulation vector. CBZ forms I and III were characterized by differential scanning calorimetry (DSC) and XRD. Powder mixtures of forms I and III at various ratios (0 - 100% w/w; form III) were subjected to XRD. Five diffraction peaks were used for the peak-area method to compare with PLS. The results obtained by PLS had a better predictive accuracy compared to those of the peak-area method. The XRD-PLS method was established as a non-destructive, non-contact way to avoid the particle orientation effect based on statistical theory.

収録刊行物

  • Analytical sciences : the international journal of the Japan Society for Analytical Chemistry

    Analytical sciences : the international journal of the Japan Society for Analytical Chemistry 24(4), 451-457, 2008-04-10

    社団法人 日本分析化学会

参考文献:  30件中 1-30件 を表示

  • <no title>

    HALEBLIAN J. K.

    J. Pharm. Sci. 58, 911, 1969

    被引用文献1件

  • <no title>

    ICH Harmonized Guideline

    Q6A Specifications, Test Procedures and Acceptance Criteria for New Drug Substances and New Drug Products, 1999

    被引用文献1件

  • <no title>

    BYRN S.

    Pharm. Res. 12, 945, 1995

    被引用文献1件

  • <no title>

    FLORENCE A. J.

    J. Pharm. Sci. 95, 1918, 2006

    被引用文献1件

  • <no title>

    PALABIYIK I. M.

    J. Pharm. Biomed. Anal. 34, 473, 2004

    被引用文献1件

  • <no title>

    KRAMER R.

    Chemometric Techniques for Quantitative Analysis, 1998

    被引用文献1件

  • <no title>

    HASEGAWA T.

    Quantitative Analytical Techniques of Spectra, 2005

    被引用文献1件

  • <no title>

    OTSUKA M.

    J. Near Infrared Spectrosc. 14, 9, 2006

    被引用文献1件

  • <no title>

    YOSHINO H.

    Chem. Pharm. Bull. 32, 1523, 1984

    被引用文献1件

  • <no title>

    ZEVIN L. S.

    Quantitative X-ray Diffractometry, 1995

    被引用文献1件

  • <no title>

    OKUMURA T.

    Colloids Surf., B 49, 153, 2006

    被引用文献1件

  • <no title>

    OKUMURA T.

    J. Pharm. Sci. 94, 1013, 2005

    被引用文献1件

  • <no title>

    UMEDA T.

    Yakuzaigaku Zasshi 104, 786, 1984

    被引用文献1件

  • <no title>

    KANENIWA N.

    Yakuzaigaku Zasshi 107, 808, 1987

    被引用文献1件

  • <no title>

    GRZESIAK A. L.

    J. Pharm. Sci. 92, 2260, 2003

    被引用文献1件

  • <no title>

    TIAN F.

    J. Pharm. Biomed. Anal. 40, 271, 2006

    被引用文献1件

  • <no title>

    HACHEY M. R. J.

    Raman Tech. for Today's Spectroscopists, 2004

    被引用文献1件

  • <no title>

    NADLER B.

    J. Chemom. 19, 45, 2005

    被引用文献1件

  • <no title>

    MCMAHON L. E.

    J. Pharm. Sci. 85, 1064-1069, 1996

    被引用文献4件

  • <no title>

    KRAHN F. U.

    Pharm. Acta Helv. 62, 247, 1987

    被引用文献1件

  • <no title>

    DUGU'E J.

    Pharm. Acta Helv. 66, 307, 1991

    被引用文献1件

  • <no title>

    CEOLIN R.

    J. Pharm. Sci. 86, 1062-1065, 1997

    被引用文献3件

  • <no title>

    MATSUDA Y.

    J. Pharm. Pharmacol. 46, 162, 1994

    被引用文献5件

  • <no title>

    RUSTICHELLI C.

    J. Pharm. Biomed. Anal. 23, 41, 2000

    被引用文献1件

  • <no title>

    PARK K.

    Cryst. Growth Des. 3, 991, 2003

    被引用文献1件

  • <no title>

    MCMAHON L. E.

    J. Pharm. Sci. 85, 1064-1069, 1996

    被引用文献4件

  • <no title>

    WOLD S.

    Chemom. Intell. Lab. Syst. 58, 131, 2001

    被引用文献1件

  • <no title>

    HELLAND I. S.

    Chemom. Intell. Lab. Syst. 58, 97, 2001

    被引用文献2件

  • <no title>

    GRAMATICA P.

    J. Chem. Inf. Comput. Sci. 44, 1794, 2004

    被引用文献1件

  • <no title>

    HASEGAWA T.

    Appl. Spectrosc. 56, 288, 2002

    被引用文献1件

各種コード

  • NII論文ID(NAID)
    10021099447
  • NII書誌ID(NCID)
    AA10500785
  • 本文言語コード
    ENG
  • 資料種別
    ART
  • ISSN
    09106340
  • NDL 記事登録ID
    9452041
  • NDL 雑誌分類
    ZP4(科学技術--化学・化学工業--分析化学)
  • NDL 請求記号
    Z54-F482
  • データ提供元
    CJP書誌  NDL  J-STAGE 
ページトップへ