Rapid Preparation of Bi2Sr2CaCu2Oy, by Using a Domestic Microwave Oven with a SiC susceptor

• Okano Yusuke

  Kanazawa Institute of Technology

• Nakamura Toshiki

  Takasago Industry Co., Ltd

• Inou Yoshitaka

  Takasago Industry Co., Ltd

• Ando Tomohiro

  Daiken Chemical Co., Ltd

• Ohhashi Kentaro

  Kanazawa Institute of Technology

Bibliographic Information

Other Title

• ＳｉＣサセプターを用いた家庭用電子レンジでのＢｉ系銅酸化物超伝導体の急速な合成
• 研究速報 SiCサセプターを用いた家庭用電子レンジでのBi系銅酸化物超伝導体の急速な合成
• ケンキュウ ソクホウ SiC サセプター オ モチイタ カテイヨウ デンシ レンジ デノ Biケイ ドウ サンカブツ チョウデンドウタイ ノ キュウソクナ ゴウセイ

Abstract

Nearly single-phase samples of high-Tc superconductors of the Bi-2212 phase have been prepared using a domestic microwave oven. Since it is to be important for the preparation to control the temperature of the sample environment, the samples were placed into thermally insulated box whose inner surface is made by SiC. An industrial microwave (2.45 GHz) furnace was used with repeating the microwave radiation processes with intermediate grinding. The comparison among microstructures of the samples obtained by domestic and industrial microwave ovens as well as those of TSFZ single crystals and polycrystals by solid state method was reported.

Journal

• Journal of the Japan Society of Powder and Powder Metallurgy

  Journal of the Japan Society of Powder and Powder Metallurgy 55 (2), 85-89, 2008

  Japan Society of Powder and Powder Metallurgy

Keywords

• Microwave radiation
• Bi-2212 superconductor
• susceptor
• SEM

Details

• CRID: 1390282681286285568
• NII Article ID: 10021172625
• NII Book ID: AN00222724
• DOI: 10.2497/jjspm.55.85
• COI: 1:CAS:528:DC%2BD1cXis1Gjtrc%3D
• ISSN: 18809014
• ISSN: 05328799
• NDL BIB ID: 9390010
• Web Site: https://ndlsearch.ndl.go.jp/books/R000000004-I9390010
• Text Lang: ja
• Data Source:
  • JaLC
  • NDL
  • Crossref
  • CiNii Articles
• Abstract License Flag: Disallowed