Preparation of Rod-like β-Si<sub>3</sub>N<sub>4</sub> Single Crystal Particles

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  • 棒状β-Si<sub>3</sub>N<sub>4</sub>単結晶粒子の作製
  • ボウジョウ ベータ Si3N4 タンケッショウ リュウシ ノ サクセイ エイブ

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Abstract

A systematic method of growing rod-like β-Si3N4 single crystals from a melt flux has been developed. β-Si3N4 particles with a diameter of 1-2μm, a length of 10-20μm and a low density of defects were obtained by heating a mixture of α-Si3N4, Y2O3 and SiO2. The residual glassy phase was removed by subsequent acid treatments.

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