Tensile Bond Strength of 4-META/MMA-TBB Resin to Ground Bovine Enamel Using a Self-etching Primer

DOI NDLデジタルコレクション Web Site PubMed 被引用文献13件 参考文献30件
  • HAYAKAWA Tohru
    Department of Dental Materials, Research Institute of Oral Science, Nihon University School of Dentistry
  • FUKUSHIMA Tadao
    Department of Dental Engineering, Biomaterials section, Fukuoka Dental College
  • NEMOTO Kimiya
    Department of Dental Materials, Research Institute of Oral Science, Nihon University School of Dentistry

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The purpose of this study was to examine the effectiveness of self-etching primer in adhering 4-META/MMA-TBB resin to bovine enamel. In this study, we designed an original self-etching primer which contained an aqueous mixture of 4-MET, 35wt% HEMA, and ferric chloride. The polished bovine enamel surface was treated with self-etching primer for 30 seconds. Tensile bond strength of 4-META/MMA-TBB resin to enamel was measured after 1-day immersion in water at 37°C. The self-etching primer containing 30wt% 4-MET and 35wt% HEMA (4MET30) gave a significantly higher bond strength of 11.2±2.8MPa than other self-etching primers. The addition of ferric chloride into 4MET30 primer significantly decreased tensile bond strength. SEM observation revealed that 4MET30 treatment produced no distinct dissolution on enamel. When compared with phosphoric acid etching, the self-etching primer containing 30wt% 4-MET and 35wt% HEMA was more superior in adhering 4-META/MMA-TBB resin to enamel.

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