Glochidionionosides A-D : Megastigmane Glucosides from Leaves of Glochidion zeylanicum (GAERTN. ) A. JUSS

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Five megastigmane glucosides were isolated from the leaves of Glochidion zeylanicum. One of them was a known compound, blumenol C O-β-D-glucopyranoside (1), and the structures of the four new compounds, glochidionionosides A—D (2—5), were mainly elucidated by spectroscopic methods, including a modified Mosher's method. The absolute configurations of the six-membered ring of glochidionionoside D (5) were deduced by β-D-glucopyranosylation-induced shift trends in the 13C-NMR spectra and confirmed by X-ray analysis as its p-bromobenzoate (5b), and the axis chirality of C-7 was determined to be R.

収録刊行物

  • Chemical & pharmaceutical bulletin

    Chemical & pharmaceutical bulletin 51(3), 286-290, 2003-03-01

    公益社団法人日本薬学会

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  • NII論文ID(NAID)
    110003615285
  • NII書誌ID(NCID)
    AA00602100
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    ENG
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    ART
  • ISSN
    00092363
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    Z53-D167
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