A New Technique to Produce Clean and Thin Silicon Films <I>In Situ</I> in a UHV Electron Microscope for TEM-TED Studies of Surfaces

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A new technique of in situ oxygen gas reaction thinning of Si films at around 750–800°C in an ultrahigh-vacuum electron microscope was developed. The technique produced films as thin as 10 to 20 nm. Such a thin film allows us to observe surface atomic steps, out-of-phase boundaries and {1/7 0}, {1/7 1/7} and {2/7 0} spots from the Si(111)7×7 surface. These spots were not observed in previous studies, having been masked by strong inelastic scattering. The technique is useful not only for detecting clear diffraction spots of kinematical intensity for surface structure analysis but also for observation of high-resolution plan-view structure images of clean and adsorbed surfaces.

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詳細情報 詳細情報について

  • CRID
    1571135652314136704
  • NII論文ID
    110003923375
  • NII書誌ID
    AA10650595
  • 本文言語コード
    en
  • データソース種別
    • CiNii Articles

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