Rapid Preparation of High-T<sub>c</sub> Superconductors of the Bi-2212 Phase Using a Domestic Microwave Oven

  • Kato Masatsune
    Department of Applied Physics, Graduate School of Engineering, Tohoku University, Aoba–yama 08, Aoba–ku, Sendai 980–8579, Japan
  • Sakakibara Kenji
    Department of Applied Physics, Graduate School of Engineering, Tohoku University, Aoba–yama 08, Aoba–ku, Sendai 980–8579, Japan
  • Koike Yoji
    Department of Applied Physics, Graduate School of Engineering, Tohoku University, Aoba–yama 08, Aoba–ku, Sendai 980–8579, Japan

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タイトル別名
  • Rapid Preparation of High-Tc Superconductors of the Bi-2212 Phase Using a Domestic Microwave Oven.

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Single-phase samples of high-Tc superconductors of the Bi-2212 phase have been prepared using a domestic microwave oven. It is to be important for the preparation to control the temperature of the sample environment and to repeat the microwave-radiation process with intermediate grinding, because the Bi-2212 phase is stable only in a narrow temperature range and requires a long heat-treatment time for formation. The partial substitution of Pb for Bi is also to be effective for the formation of the Bi-2212 phase.

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