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The stereoselective synthesis of the 1-O-α-D-glucopyranosides and l-O-α-D-cellobiosides of 3-deoxy-2(R)- and 2(S)-glycerols to determine the complete stereochemistry of rhynchosporoside, which is a host selective phytotoxin from Rhynchosporium secalis, is described in detail.
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