SIMPLE EXTRACTION OF 1-PHENYLETHYLAMINE IN HUMAN URINE BY HEADSPACE SOLID PHASE MICROEXTRACTION (SPME)

• Ishii, Akira

• Seno, Hiroshi

• Guan, Fuyu

• Watanabe, Kanako

• Kumazawa, Takeshi

• Hattori, Hideki

• Suzuki, Osamu

書誌事項

タイトル別名

• ヘッドスペース固相ミクロ抽出（SPME)法による1-フェニルニチルアミンのヒト尿からの簡便抽出法

抄録

A method for simple clean-up of 1-phenylethylamine (1-PEA. α-phenylethylamine. α-methylbenzylamine). a possible abused drug. in human urine by headspace solid phase microextraction (SPME) with a polydimethylsiloxane-divinylbenzene fiber. is presented. Quantitation was made by capillary gas chromatography with nitrogen-phosphorus detection and β-methylphenethylamine was used as internal standard (IS). The recoveries of 1-PEA and IS were 4.75 to 8.93% and 13.4%. respectively. The calibration curve for 1-PEA was linear in the range of 25-500 ng/ml urine. The detection limit was about 20 ng/ml urine.

収録刊行物

• 法中毒

  法中毒 15 (3), 189-193, 1997-09-16

  日本法中毒学会

キーワード

• 1-Phenylethylamine

詳細情報

• CRID: 1050282676645742848
• NII論文ID: 120005314029
• ISSN: 09159606
• HANDLE: 10271/1713
• Web Site: https://hama-med.repo.nii.ac.jp/records/1680
• 本文言語コード: en
• 資料種別: journal article
• データソース種別:
  • IRDB
  • CiNii Articles