書誌事項
- タイトル別名
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- Determination of organo-tin compounds by gas-liquid chromatography
- ユウキ スズ カゴウブツ ノ ガス クロマトグラフィー ニ ヨル ブンセキ
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An improved method was proposed for the gasliquid chromatographic determination of n-butyl-, n-octyl- and phenyl-tin halogenides, which were treated with Grignard reagents before injection into a gas-liquid chromatograph equipped with a thermal conductivity detector. Grignard reagents and gasliquid chromatographic conditions used in this procedure were as follows.<BR>Butyl-tin compounds: Grignard reagent-n-propyl magnesium bromide; column-3 mm × 0.75 m, stainless steel packed with 25 wt.% silicone DC 550 on 80-to 100-mesh Celite 545; temperature -190°C; carrier gas-helium 50 ml per min. flow rate; internal standard-n-octadecane.<BR>Octyl-tin compounds : Grignard reagent-n-amyl magnesium bromide; column-3 mm × 0.75 m, stainless steel packed with 25 wt.% silicone DC HV grease on 80- to 100-mesh Celite 545; temperature -280°C; carrier gas-helium 90 ml per min. flow rate; internal standard-trioctylpropyl-tin.<BR>Phenyl-tin compounds: Grignard reagent-n-amyl magnesium bromide; column-3 mm × 0.75m, stainless steel packed with 25 wt.% silicone DC HV grease on 80- to 100-mesh Celite 545; temperature -260°C; carrier gas-helium 50 ml per min. flow rate; internal standard-triphenylbutyl-tin.
収録刊行物
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- 分析化学
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分析化学 18 (2), 169-175, 1969
公益社団法人 日本分析化学会
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詳細情報 詳細情報について
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- CRID
- 1390001204660144640
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- NII論文ID
- 130000944102
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- NII書誌ID
- AN00222633
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- NDL書誌ID
- 8443214
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- ISSN
- 05251931
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- 本文言語コード
- ja
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- データソース種別
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- JaLC
- NDL
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- 抄録ライセンスフラグ
- 使用不可