Low Temperature Aging and Repeated Strain Aging in Ni Maraging Steels

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The hardening mechanism of Ni maraging steels on aging and on repeated strain aging has been investigated by means of specific heat, electrical resistivity and hardness measurements, etc. On aging in the temperature range from 600 to 800 K, Mo rich zones are formed prior to the precipitation of Ni3Mo, leading to the pronounced hardening in Ni maraging steels. These zones are considered to transform to Ni3Mo by the in situ type process in the later aging stage. At the aging temperature below 720 K, however, this transformation does not proceed in the hardening stage but occurs in the over aging stage.<BR>Repetition of low temperature aging and cold working (repeated strain aging) leads to the acceleration of formation of Mo rich zones, resulting in a rapid increase in tensile strength. For example, the tensile strength of a specimen with the 10 cycles repetition of the 748 K–120 s aging and 5% cold working reaches 1700 MPa, which exceeds the highest tensile strength of 1500 MPa attained by the 748 K–36 ks aging. This suggests that Mo rich zones are fromed on dislocations, and that the dislocations released (or newly generated) by the cold working on the above treatment can again supply the nucleation sites for the next formation of Mo rich zones.

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