Crystal Structure of 4-Phenyl-piperazine-1-sulfonamide

• BERREDJEM Malika

  LCOA, Bioorganique Chemistry Group, Sciences Faculty, Chemistry Départment, Badji Mokhar-Annaba University Laboratoire CSPBAT, FRE 3043 CNRS, University of Paris 13

• BOUASLA Radia

  LCOA, Bioorganique Chemistry Group, Sciences Faculty, Chemistry Départment, Badji Mokhar-Annaba University

• AOUF Nour-Eddine

  LCOA, Bioorganique Chemistry Group, Sciences Faculty, Chemistry Départment, Badji Mokhar-Annaba University

• BARBEY Carole

  Laboratoire CSPBAT, FRE 3043 CNRS, University of Paris 13

抄録

The structure of 4-phenyl-piperazine-1-sulfonamide was determined by X-ray crystallography. The compound crystallized in a monoclinic system and was characterized as follows: P2₁/c, a = 24.1829(7), b = 9.5485(3), c = 9.7885(2)Å, β = 92.2337(16)°, Z = 8, V = 2258.55(11)ų. The crystal structure was solved by direct methods and refined by full-matrix least-squares on F² to final values of R1 = 0.0427 for 3206 reflections [I > 2σ(I)] and R1 = 0.0739, wR2 = 0.1083 for all the 4589 unique reflections. The crystal structure consists of layers of polar regions that enclose a sulfonamide function linked by hydrogen bonds and hydrophobic regions with π-π stacking interactions.

収録刊行物

• X-ray Structure Analysis Online

  X-ray Structure Analysis Online 26 13-14, 2010

  社団法人 日本分析化学会

キーワード

• Materials Chemistry
• Analytical Chemistry

詳細情報

• CRID: 1390001205300172544
• NII論文ID: 130004953575
• DOI: 10.2116/xraystruct.26.13
• ISSN: 18833578
• Web Site: http://www.jstage.jst.go.jp/article/xraystruct/26/0/26_0_13/_pdf
• 本文言語コード: en
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