Repetitive‐Synthesis of Bulky Dendrimers – A Reversibly Photoactive Dendrimer with Six Azobenzene Side Chains

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<jats:title>Abstract</jats:title><jats:p>Dendrimers with bulky repeating units containing up to 43 benzene rings (in <jats:bold>9</jats:bold>) have been obtained by using a repetitive divergent synthetic strategy (three generations). The new functional dendrimer <jats:bold>13</jats:bold> containing six azobenzene units at the periphery was synthesized allowing a reversible switching of the shape and size of the molecule upon irradiation. An X‐ray structure analysis of the dendritic molecule <jats:bold>3a</jats:bold> shows the inclusion of acetonitrile.</jats:p>

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