Facile Synthesis of Fe<sub>3</sub>O<sub>4</sub> Nanoparticles with a High Specific Surface Area

  • Ma Jianchao
    College of mining Technology, Taiyuan University of Technology
  • Wang Lingling
    College of mining Technology, Taiyuan University of Technology
  • Wu Yanli
    Key Laboratory of Coal Science and Technology (Taiyuan University of Technology), Ministry of Education and Shanxi Province
  • Dong Xianshu
    College of mining Technology, Taiyuan University of Technology
  • Ma Qingliang
    Key Laboratory of Coal Science and Technology (Taiyuan University of Technology), Ministry of Education and Shanxi Province
  • Qiao Chen
    College of Chemistry and Chemical Engineering, Taiyuan University of Technology
  • Zhang Qingfang
    College of Chemistry and Chemical Engineering, Taiyuan University of Technology
  • Zhang Jilong
    College of mining Technology, Taiyuan University of Technology

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Other Title
  • Facile Synthesis of Fe₃O₄ Nanoparticles with a High Specific Surface Area

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Abstract

A facile method was developed for the synthesis of Fe3O4 nanoparticles with a higher specific surface area. Na2CO3 and hydrazine were added during the co-precipitation of ferrous and ferric species, without the assistance of any organic reagents or templates. The results show that the prepared Fe3O4 nanoparticles had a specific surface area of 286.9 m2/g, with satisfactory size and purity, thus exhibiting superparamagnetic properties with a relatively strong saturation magnetization (91 emu/g) at room temperature. This method is inexpensive, nontoxic, and reproducible.

Journal

  • MATERIALS TRANSACTIONS

    MATERIALS TRANSACTIONS 55 (12), 1900-1902, 2014

    The Japan Institute of Metals and Materials

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