Development of an adiabatic low-temperature microcalorimeter and thermal study on low-temperature behavior of protein crystals 断熱型ミクロカロリメータの開発および蛋白質結晶の低温挙動に関する熱的研究
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Bibliographic Information
- Title
-
Development of an adiabatic low-temperature microcalorimeter and thermal study on low-temperature behavior of protein crystals
- Other Title
-
断熱型ミクロカロリメータの開発および蛋白質結晶の低温挙動に関する熱的研究
- Author
-
宮崎, 裕司
- Author(Another name)
-
ミヤザキ, ユウジ
- University
-
大阪大学
- Types of degree
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博士 (理学)
- Grant ID
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甲第4645号
- Degree year
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1993-03-25
Note and Description
博士論文
Table of Contents
- Abstract / (0002.jp2)
- Development of an Adiabatic Low-temperature Microcalorimeter and Thermal Study on Low-temperature Behavior of Protein Crystals / (0002.jp2)
- Contents / (0003.jp2)
- Chapter1.General Introduction / p1 (0004.jp2)
- §1-1.Glassy State / p1 (0004.jp2)
- §1-2.Protein as Glass-like Substance / p4 (0006.jp2)
- §1-3.Aim of Present Study / p6 (0007.jp2)
- References to Chapter1 / p7 (0007.jp2)
- Chapter2.Construction of an Adiabatic Low-temperature Microcalorimeter / p8 (0008.jp2)
- §2-1.Introduction / p8 (0008.jp2)
- §2-2.Principle / p9 (0008.jp2)
- 2-2-1.Adiabatic Heat Capacity Measurement / p9 (0008.jp2)
- 2-2-2.Temperature Measurement / p11 (0009.jp2)
- §2-3.Construction of Apparatus / p15 (0011.jp2)
- 2-3-1.Cryostat / p15 (0011.jp2)
- 2-3-2.Sample Cell / p15 (0011.jp2)
- 2-3-3.Measurement and Adiabatic Control Circuit / p17 (0012.jp2)
- §2-4.Precision and Accuracy of Apparatus / p21 (0014.jp2)
- 2-4-1.Temperature Measurement / p21 (0014.jp2)
- 2-4-2.Heat Capacity Measurement of Sample Cell / p23 (0015.jp2)
- 2-4-3.Heat Capacity Measurement of Calorimetric Standard Benzoic Acid / p23 (0015.jp2)
- References to Chapter2 / p32 (0020.jp2)
- Chapter3.Low-temperature Behavior of Tetragonal Egg-white Lysozyme Crystal / p33 (0020.jp2)
- §3-1.Introduction / p33 (0020.jp2)
- §3-2.Experimental / p34 (0021.jp2)
- 3-2-1.Sample Preparation / p34 (0021.jp2)
- 3-2-2.Heat Capacity Measurement / p34 (0021.jp2)
- §3-3.Results / p37 (0022.jp2)
- §3-4.Discussion / p62 (0035.jp2)
- 3-4-1.Fusion of Water in Crystal / p62 (0035.jp2)
- 3-4-2.Glass-like Behavior / p64 (0036.jp2)
- 3-4-3.Relation between Lysozyme Dynamics and Crystal Water / p64 (0036.jp2)
- References to Chapter3 / p84 (0046.jp2)
- Chapter4.Low-temperature Behavior of Monoclinic Horse Myoglobin Crystal / p86 (0047.jp2)
- §4-1.Introduction / p86 (0047.jp2)
- §4-2.Experimental / p88 (0048.jp2)
- 4-2-1.Sample Preparation / p88 (0048.jp2)
- 4-2-2.Heat Capacity Measurement / p90 (0049.jp2)
- §4-3.Results / p92 (0050.jp2)
- §4-4.Discussion / p122 (0065.jp2)
- 4-4-1.Fusion of Water in Myoglobin Crystal / p122 (0065.jp2)
- 4-4-2.Glass Transition / p124 (0066.jp2)
- 4-4-3.Analysis of Relaxation Time / p134 (0071.jp2)
- 4-4-4.Relation between Myoglobin Dynamics and Crystal Water / p135 (0071.jp2)
- References to Chapter4 / p156 (0082.jp2)
- Chapter5.Conclusion / p158 (0083.jp2)
- References to Chapter5 / p160 (0084.jp2)