Preparation and surface properties of polysiloxanes with fluorocarbon side-chains フルオロカーボンを側鎖に有するシロキサン高分子の合成と界面物性

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著者

    • 小林, 秀樹 コバヤシ, ヒデキ

書誌事項

タイトル

Preparation and surface properties of polysiloxanes with fluorocarbon side-chains

タイトル別名

フルオロカーボンを側鎖に有するシロキサン高分子の合成と界面物性

著者名

小林, 秀樹

著者別名

コバヤシ, ヒデキ

学位授与大学

早稲田大学

取得学位

博士 (工学)

学位授与番号

乙第932号

学位授与年月日

1993-02-12

注記・抄録

博士論文

目次

  1. CONTENTS / p3 (0005.jp2)
  2. CHAPTER1 INTRODUCTION / p1 (0008.jp2)
  3. 1.1.Surface Characteristics of Silicone Polymers / p1 (0008.jp2)
  4. 1.2.Surface Tension Measurement / p2 (0009.jp2)
  5. 1.3.Surface Active Materials Based on Silicone Polymers / p5 (0012.jp2)
  6. CHAPTER2 SYNTHESIS AND CHARACTERIZATION OF POLY[(3,3,4,4,5,5,6,6,6-NONAFLUOROHEXYL)METHYLSILOXANE] / p7 (0014.jp2)
  7. 2.1.Structural Features of Fluorosilicone Polymers / p7 (0014.jp2)
  8. 2.2.Cationic Polymerization / p8 (0015.jp2)
  9. 2.3.Contact Angle Measurement / p10 (0017.jp2)
  10. 2.4.Solid Surface Tension of PTFPMS and PNFHMS / p11 (0018.jp2)
  11. 2.5.Comparison with Other Fluoro Polymers / p14 (0021.jp2)
  12. 2.6.Summary / p16 (0023.jp2)
  13. CHAPTER3 SYNTHESIS AND CHARACTERIZATION OF POLY[(1H,1H,2H,2H-HEPTADECAFLUORODECYL)METHYLSILOXANE] / p18 (0025.jp2)
  14. 3.1.Previous Study on PHDFDMS / p18 (0025.jp2)
  15. 3.2.Condensation Polymerization of PHDFDMS / p19 (0026.jp2)
  16. 3.3.Characterization of PHDFDMS / p20 (0027.jp2)
  17. 3.4.Surface Tension of the PHDFDMS / p21 (0028.jp2)
  18. 3.5.Summary / p27 (0034.jp2)
  19. CHAPTER4 LIQUID SURFACE TENSION OF FLUORINATED POLYSILOXANE FLUIDS / p29 (0036.jp2)
  20. 4.1.Liquid Surface Tension Determination / p29 (0036.jp2)
  21. 4.2.LeGrand and Gaines Equation / p30 (0037.jp2)
  22. 4.3.Preparation of Fluorosilicone Fluids / p33 (0040.jp2)
  23. 4.4.Liquid Surface Tension of Fluorosilicone Fluids / p33 (0040.jp2)
  24. 4.5.Thermal Properties / p36 (0043.jp2)
  25. 4.6.Summary / p39 (0046.jp2)
  26. CHAPTER5 SYNTHESIS AND CHARACTERIZATION OF POLY(3,3,3-TRIFLUORO-PROPYL SILSESQUIOXANE)AND POLY(3,3,4,4,5,5,6,6,6-NONAFLUOROHEXYL SILSESQUIOXANE) / p41 (0048.jp2)
  27. 5.1.Polymers from Fluoroalkyl Trifunctional Silanes / p41 (0048.jp2)
  28. 5.2.Preparation of Polysilsesquioxanes / p42 (0049.jp2)
  29. 5.3.Characterization of Polysilsesquioxanes / p43 (0050.jp2)
  30. 5.4.Condensation Cure Technique / p46 (0053.jp2)
  31. 5.5.Solid Surface Tension of Polysilsesquioxanes / p46 (0053.jp2)
  32. 5.6.Comparison with Self-Assembled Monolayers / p49 (0056.jp2)
  33. 5.7.Comparison with Linear Polysiloxanes / p50 (0057.jp2)
  34. 5.8.Summary / p51 (0058.jp2)
  35. CHAPTER6 SYNTHESIS AND CHARACTERIZATION OF POLY(3,3,3-TRIFLUORO-PROPYLMETHYLSILOXANE-CO-DIMETHYLSILOXANE)GUM / p53 (0060.jp2)
  36. 6.1.Fluorosilicone-Based Rubbers / p53 (0060.jp2)
  37. 6.2.Equilibrium Copolymerization / p54 (0061.jp2)
  38. 6.3.Sequential Living Polymerization / p55 (0062.jp2)
  39. 6.4.Microstrue Analyzed by 29Si-NMR / p57 (0064.jp2)
  40. 6.5.Low Temperature Property / p59 (0066.jp2)
  41. 6.6.Polymer Blend / p61 (0068.jp2)
  42. 6.7.Summary / p63 (0070.jp2)
  43. CHAPTER7 SURFACE TREATMENT OF FUMED SILICA WITH HEXAMETHYL-DISILAZANE AND OLIGODIMEYHYLSILOXANE-α,ω-DIOL / p65 (0072.jp2)
  44. 7.1.Surface Modification of Fumed Silica / p65 (0072.jp2)
  45. 7.2.Silica Silanol Titration Method / p66 (0073.jp2)
  46. 7.3.Silica Surface Treatment with HMDZ / p67 (0074.jp2)
  47. 7.4.Silica Surface Treatment with OHDMS / p70 (0077.jp2)
  48. 7.5.Hydrophpbicity of Treated Silica / p76 (0083.jp2)
  49. 7.6.Antifoaming Compounds / p77 (0084.jp2)
  50. 7.7.Summary / p78 (0085.jp2)
  51. CHAPTER8 SURFACE TREATMENT OF SUPERPARAMAGNETIC MAGNETITE PARTICLES WITH FUNCTIONAL AMINO-SILANE / p80 (0087.jp2)
  52. 8.1.Amino-Silane Coupling Agent / p80 (0087.jp2)
  53. 8.2.Magnetic Particles / p81 (0088.jp2)
  54. 8.3.Amino-Silane Treatment / p85 (0092.jp2)
  55. 8.4.Enzyme Immobilization and Activity / p87 (0094.jp2)
  56. 8.5.Summary / p90 (0097.jp2)
  57. CHAPTER9 FLUOROSILICONE SURFACTANTS / p92 (0099.jp2)
  58. 9.1.Type of Surfactants / p92 (0099.jp2)
  59. 9.2.Preparation of Fluorosilicone Surfactants / p93 (0100.jp2)
  60. 9.3.Equilibrium Surface Tension / p97 (0104.jp2)
  61. 9.4.Dynamic Surface Tension / p100 (0107.jp2)
  62. 9.5.Wettability Tests / p101 (0108.jp2)
  63. 9.6.Summary / p102 (0109.jp2)
  64. CHAPTER10 FLUOROSILICONE ANTIFOAMS / p105 (0112.jp2)
  65. 10.1.Aqueous Antifoams / p105 (0112.jp2)
  66. 10.2.Aqueous solutions of Foaming Surfactants / p106 (0113.jp2)
  67. 10.3.Preparation of Fluorinated Polysiloxanes / p107 (0114.jp2)
  68. 10.4.Preparation of Antifoam Agents / p109 (0116.jp2)
  69. 10.5.Performance of Antifoaming Agents / p110 (0117.jp2)
  70. 10.6.Summary / p115 (0122.jp2)
  71. CHAPTER11 GENERAL CONCLUSION / p117 (0124.jp2)
  72. LIST OF PUBLICATIONS / (0127.jp2)
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各種コード

  • NII論文ID(NAID)
    500000097435
  • NII著者ID(NRID)
    • 8000000097664
  • DOI(NDL)
  • NDL書誌ID
    • 000000261749
  • データ提供元
    • NDL-OPAC
    • NDLデジタルコレクション
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