Development of off-line and on-line preconcentration techniques for trace elements and their determination with inductively coupled plasma mass spectrometry オフ・ライン及びオン・ラインでの微量元素の前濃縮法の開発とそれに基づくICP質量分析計による定量
この論文にアクセスする
この論文をさがす
著者
書誌事項
- タイトル
-
Development of off-line and on-line preconcentration techniques for trace elements and their determination with inductively coupled plasma mass spectrometry
- タイトル別名
-
オフ・ライン及びオン・ラインでの微量元素の前濃縮法の開発とそれに基づくICP質量分析計による定量
- 著者名
-
Shabani, Mohammad Bagher
- 著者別名
-
シャバニー, モハマッド バゲール
- 学位授与大学
-
東京大学
- 取得学位
-
博士 (理学)
- 学位授与番号
-
甲第9228号
- 学位授与年月日
-
1991-09-30
注記・抄録
博士論文
目次
- CONTENTS / p6 (0007.jp2)
- CHAPTER I.INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY / p1 (0014.jp2)
- I-1.INTRODUCTION / p2 (0015.jp2)
- I-2.Detection Limits,Dynamic Range and Analytical Precision / p4 (0017.jp2)
- I-3.Spectral Overlaps / p7 (0020.jp2)
- I-4.Isobaric Spectral Overlaps / p7 (0020.jp2)
- I-5.Background Spectral Feature / p8 (0021.jp2)
- I-6.Oxide,Hydroxide,and Doubly Charged Analyte Species / p11 (0024.jp2)
- I-7.Nonspectral Matrix Effects / p11 (0024.jp2)
- I-8.Errors Minimization Approaches / p12 (0025.jp2)
- REFERENCES / p13 (0026.jp2)
- CHAPTER II.DETERMINATION OF TRACE LANTHANIDES AND YTTRIUM IN SEAWATER BY INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY AFTER PRECONCENTRATION WITH SOLVENT EXTRACTION AND BACK-EXTRACTION / p16 (0029.jp2)
- II-1.INTRODUCTION / p17 (0030.jp2)
- II-2.EXPERIMENTAL SECTION / p19 (0032.jp2)
- II-3.RESULTS AND DISCUSSION / p25 (0038.jp2)
- II-4.CONCLUSION / p36 (0049.jp2)
- REFERENCES / p40 (0053.jp2)
- CHAPTER III.SAMPLE INTRODUCTION BY ON-LINE TWO-STAGE SOLVENT EXTRACTION AND BACK-EXTRACTION TO ELIMINATE MATRIX INTERFERENCE AND TO ENHANCE SENSITIVITY IN THE DETERMINATION OF RARE EARTH ELEMENTS WITH INDUCTIVELY COUPLED MASS SPECTROMETRY / p42 (0055.jp2)
- III-1.INTRODUCTION / p43 (0056.jp2)
- III-2.EXPERIMENTAL SECTIONS / p45 (0058.jp2)
- III-3.RESULTS AND DISCUSSION / p51 (0064.jp2)
- III-4.CONCLUSION / p70 (0083.jp2)
- REFERENCES / p72 (0085.jp2)
- CHAPTER IV.DEVELOPMENT OF ON-LINE TOW-STAGE SOLVENT EXTRACTION AND BACK-EXTRACTION TO REDUCE OXIDE INTERFERENCE AND TO SOLVE DYNAMIC RANGE PROBLEM IN DETERMINATION OF RARE EARTH ELEMENTS WITH INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY / p75 (0088.jp2)
- IV-1.INTRODUCTION / p76 (0089.jp2)
- IV-2.EXPERIMENTAL SECTION / p78 (0091.jp2)
- IV-3.RESULTS AND DISCUSSION / p79 (0092.jp2)
- IV-4.SUMMARY / p96 (0109.jp2)
- REFERENCES / p97 (0110.jp2)
- CHAPTER V.RAPID CONCENTRATION OF TRACE OF RARE EARTH ELEMENTS IN SEAWATER BY COMPLEXATION WITH BIS(2-ETHYLHEXYL)HYDROGEN PHOSPHATE AND 2-ETHYL DIHYDROGEN PHOSPHATE ADSORBED ON C₁₈ CARTRIDGE AND DETERMINATION BY INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY / p99 (0112.jp2)
- V-I.INTRODUCTION / p100 (0113.jp2)
- V-2.EXPERIMENTAL SECTION / p103 (0116.jp2)
- V-3.RESULTS AND DISCUSSION / p108 (0121.jp2)
- V-4.CONCLUSION / p125 (0138.jp2)
- REFERENCES / p130 (0143.jp2)
- CHAPTER VI.DETERMINATION OF TRACE RARE EARTH ELEMENTS IN SEAWATER BY INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY WITH ON-LINE PREC0NCENTRATION / p133 (0146.jp2)
- VI-1.INTRODUCTION / p134 (0147.jp2)
- VI-2.EXPERIMENTAL SECTION / p136 (0149.jp2)
- VI-3.RESULTS AND DISCUSSION / p140 (0153.jp2)
- VI-4.CONCLUSIONS / p162 (0176.jp2)
- REFERENCES / p164 (0178.jp2)
- CHAPTER VII.DETERMINATION OF TRACE RHENIUM IN SEAWATER BY INDUCTIVELY COUPLED PLASMA MASS SPECTROMETRY WITH ON-LINE PRECONCENTRATION / p166 (0180.jp2)
- VII-1.INTRODUCTION / p167 (0181.jp2)
- VII-2.EXPERIMENTAL SECTION / p169 (0183.jp2)
- VII-3.RESULTS AND DISCUSSION / p174 (0188.jp2)
- VII-4.CONCLUSION / p184 (0198.jp2)
- REFERENCES / p185 (0199.jp2)
- CHAPTER VIII.FUTURE IMPROVEMENTS AND PROSPECTS / p187 (0201.jp2)