Electrochemical approach to the syntheses of fluorinated heterocycles 電気化学的手法を用いる含フッ素複素環の合成

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著者

    • 小林, 政史 コバヤシ, マサフミ

書誌事項

タイトル

Electrochemical approach to the syntheses of fluorinated heterocycles

タイトル別名

電気化学的手法を用いる含フッ素複素環の合成

著者名

小林, 政史

著者別名

コバヤシ, マサフミ

学位授与大学

岡山大学

取得学位

博士 (工学)

学位授与番号

甲第1472号

学位授与年月日

1996-03-25

注記・抄録

博士論文

目次

  1. Contents / p1 (0003.jp2)
  2. Chapter1 General Introduction. / (0004.jp2)
  3. 1.1 General Introduction / p2 (0004.jp2)
  4. 1.3 General Preparations of Fluorinated Benzimidazoles / p14 (0010.jp2)
  5. 1.4 An Approach to α,α-Difluoroalkylated Aromatic Compounds / p16 (0011.jp2)
  6. 1.5 General Summary / p19 (0013.jp2)
  7. 1.6 References / p21 (0014.jp2)
  8. Chapter2 Syntheses of Fluorinated Imidamides. / (0017.jp2)
  9. 2.1 Introduction / p28 (0017.jp2)
  10. 2.2 Preparation of N,N'-Disubstituted Imidamides / p29 (0018.jp2)
  11. 2.3 Experimental Section / p34 (0020.jp2)
  12. 2.4 References and Notes / p46 (0026.jp2)
  13. Chapter3 Oxidation of Fluorinated Imidamides Part1.Electrochemistry of Fluorinated Imidamides and An Approach to Fluorinated Benzimidazoles. / (0027.jp2)
  14. 3.1 Introduction / p48 (0027.jp2)
  15. 3.2 Chemical Oxidation of Imidamides / p52 (0029.jp2)
  16. 3.4 Electrochemical Preparation of 2-(Perfluoroalkyl)benzimidazoles / p66 (0036.jp2)
  17. 3.5 Conclusion / p67 (0037.jp2)
  18. 3.6 Experimental Section / p67 (0037.jp2)
  19. 3.7 References and Notes / p76 (0041.jp2)
  20. Chapter4 Elrctrochemistry of Trifluoroethanimidamides Part2.Electrochemical Formation and Behabior of p-Benzoquinone Imines. / (0043.jp2)
  21. 4.1 Introduction / p80 (0043.jp2)
  22. 4.2 Electrosynthesis of p-Benzoquinone Imines in Aqueous Acetonitrile / p81 (0044.jp2)
  23. 4.3 Electrochemical Behabior of p-Benzoquinone Imines / p82 (0044.jp2)
  24. 4.4 Experimental Section / p85 (0046.jp2)
  25. 4.5 References and Notes / p89 (0048.jp2)
  26. Chapter5 Cyclizations of p-Benzoquinone Imines Part1.Syntheses of Trifluoromethylated 6-Hydroxybenzimidazoles. / (0049.jp2)
  27. 5.1 Introduction / p92 (0049.jp2)
  28. 5.2 Lewis Acid Catalyzed Cyclization of p-Benzoquinone Imines / p92 (0049.jp2)
  29. 5.3 Experimental Section / p96 (0051.jp2)
  30. 5.4 References and Notes / p101 (0054.jp2)
  31. Chapter6 Cyclizations of p-Benzoquinone Imines Part 2.Syntheses of Trifluoromethylated Spirodienone Diazacarbocycles. / (0055.jp2)
  32. 6.1 Introduction / p104 (0055.jp2)
  33. 6.2 Thermal Electrocyclic Reaction of p-Benzoquinone Imines / p105 (0056.jp2)
  34. 6.3 Experimental Section / p109 (0058.jp2)
  35. 6.4 References and Notes / p116 (0061.jp2)
  36. Chapter7 Cyclizations of p-Benzoquinone Imines Part3.Electrochemical Oxidation of 2-Substituted 3-N-(Arylamino)-4,4,4-trifluoro-2-butenate:An Access to 3-Substituted 2-(Trifluoromethyl)-3H-indoles. / (0062.jp2)
  37. 7.1 Introduction / p118 (0062.jp2)
  38. 7.2 Syntheses of the Substrates / p119 (0063.jp2)
  39. 7.3 Electrochemical Preparation of p-Benzoquinone Imine Derivatives / p120 (0063.jp2)
  40. 7.4 Transformations to 2-(Trifluoromethyl)-3H-indoles / p121 (0064.jp2)
  41. 7.5 Experimental Section / p123 (0065.jp2)
  42. 7.6 References / p129 (0068.jp2)
  43. Chapter8 Reductive Defluorination of Trifluoromethyl Compounds. / (0069.jp2)
  44. 8.1 Introduction / p132 (0069.jp2)
  45. 8.2 Reduction of 2-(Trifluoromethyl)benzimidazole / p134 (0070.jp2)
  46. 8.3 Electroreduction of 2-(Trifluoromethyl)benzimidazole / p135 (0071.jp2)
  47. 8.4 Electroreduction of 2-(Trifluoromethyl)benzimidazole in the Presence of Electrophiles / p137 (0072.jp2)
  48. 8.5 Experimental Section / p138 (0072.jp2)
  49. 8.6 References / p141 (0074.jp2)
  50. Publication List / (0074.jp2)
  51. Acknowledgments / (0075.jp2)
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各種コード

  • NII論文ID(NAID)
    500000130745
  • NII著者ID(NRID)
    • 8000000954487
  • DOI(NDL)
  • 本文言語コード
    • jpn
  • NDL書誌ID
    • 000000295059
  • データ提供元
    • 機関リポジトリ
    • NDL-OPAC
    • NDLデジタルコレクション
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